The safe and controlled oxidation of thioanisole with 50 wt. % hydrogen peroxide
Abstract
This application note demonstrates the oxidation of thioanisole using hydrogen peroxide in continuous flow. It highlights the use of 50 wt% hydrogen peroxide which can be pumped neat with Vapourtec systems. Both cooled and heated conditions were explored for this exothermic reaction. The reaction temperature was controlled using a Vapourtec cooling module for the sub-ambient conditions. To explore the highest possible throughput, mildly heated conditions were also explored.
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